n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

Base Information

Chemical Name:n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide
CAS No.:415911-38-5
Molecular Formula:C₂₃H₂₇N₅O₃S
Molecular Weight:453.565
Hs Code.:

Synonyms:n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

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Chemical Property of n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

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Technology Process of n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

There total 4 articles about n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 415911-41-0
4,6-dimethyl-2-(4-{2-[({[(4-methylphenyl)sulfonyl]amino}carbonyl)amino]ethyl}anilino)-3-nitropyridine

: 415911-38-5
n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; for 4h; under 2942.29 Torr;

Reference yield:

: 415911-39-6
3-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}propanoic Acid

: 415911-38-5
n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane

2: N,N-dimethyl-formamide

3: Pd-C / methanol

With diphenyl phosphoryl azide; triethylamine; Pd-C; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 35418-07-6
methyl 3-(4-aminophenyl)propionate

: 415911-38-5
n-{[(2-{4-[(3-amino-4,6-dimethyl-2-pyridinyl)amino]phenyl}ethyl)amino]carbonyl}-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; N-ethyl-N,N-diisopropylamine / methanol; dimethyl sulfoxide

2: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane

3: N,N-dimethyl-formamide

4: Pd-C / methanol

With sodium hydroxide; diphenyl phosphoryl azide; triethylamine; N-ethyl-N,N-diisopropylamine; Pd-C; In 1,4-dioxane; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;