phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

Base Information

Chemical Name:phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate
CAS No.:415911-40-9
Molecular Formula:C₂₂H₂₂N₄O₄
Molecular Weight:406.441
Hs Code.:

Synonyms:phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

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Chemical Property of phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

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Technology Process of phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

There total 3 articles about phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 415911-39-6
3-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}propanoic Acid

: 108-95-2,27073-41-2
phenol

: 415911-40-9
phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In 1,4-dioxane; at 120 ℃; Heating / reflux;

Reference yield:

: 415911-39-6
3-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}propanoic Acid

: 108-95-2,27073-41-2
phenol

: 415911-40-9
phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In 1,4-dioxane;

Reference yield:

: 35418-07-6
methyl 3-(4-aminophenyl)propionate

: 415911-40-9
phenyl 2-{4-[(4,6-Dimethyl-3-nitro-2-pyridinyl)amino]phenyl}ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; N-ethyl-N,N-diisopropylamine / methanol; dimethyl sulfoxide

2: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane

With sodium hydroxide; diphenyl phosphoryl azide; triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dimethyl sulfoxide;