2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester

Base Information

Chemical Name:2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester
CAS No.:336195-59-6
Molecular Formula:C₂₉H₃₄Cl₂O₈
Molecular Weight:581.49
Hs Code.:

2,6-dichloro-heptanedioic acid bis-(3-<i>tert</i>-butyl-5-formyl-4-hydroxy-phenyl) ester

Synonyms:2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester

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Chemical Property of 2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester

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Technology Process of 2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester

There total 5 articles about 2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1948-33-0
tert-butylhydroquinone

: 336195-59-6
2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-dimethylaminopyridine; imidazole / CH₂Cl₂ / 3 h / 20 °C

2.1: 2,6-lutidine / SnCl₄ / toluene / 0.33 h / 20 °C

2.2: toluene / 12 h / 100 °C

3.1: 37 g / TBAF / tetrahydrofuran / 2 h / 20 °C

4.1: 4-dimethylaminopyridine; imidazole / CH₂Cl₂ / 0.5 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; tetrabutyl ammonium fluoride; tin(IV) chloride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja005867b

Reference yield:

: 155135-23-2
2-(1,1-dimethylethyl)-4-(triisopropylsilyloxy)phenol

: 336195-59-6
2,6-dichloro-heptanedioic acid bis-(3-tert-butyl-5-formyl-4-hydroxy-phenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,6-lutidine / SnCl₄ / toluene / 0.33 h / 20 °C

1.2: toluene / 12 h / 100 °C

2.1: 37 g / TBAF / tetrahydrofuran / 2 h / 20 °C

3.1: 4-dimethylaminopyridine; imidazole / CH₂Cl₂ / 0.5 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; tetrabutyl ammonium fluoride; tin(IV) chloride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja005867b