4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

Base Information

Chemical Name:4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine
CAS No.:89073-55-2
Molecular Formula:C₁₉H₂₃N₅O₄S₂
Molecular Weight:449.555
Hs Code.:

Synonyms:4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

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Chemical Property of 4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

Chemical Property:

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Technology Process of 4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

There total 6 articles about 4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-90-0
Thiomorpholin

: 89073-47-2
4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)benzenesulfonic acid

: 89073-55-2
4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

Guidance literature:: With thionyl chloride; In water; N,N-dimethyl-formamide;

Reference yield:

: 52998-22-8
5,6-diamino-1,3-diethyluracil

: 89073-55-2
4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

Guidance literature:: Multi-step reaction with 4 steps

1: ethyl <3-(dimethylamino)propyl>carbodiimide (EDAC) / H₂O

2: 30percent aq. KOH / 0.17 h / Heating

3: SOCl₂ / dimethylformamide / 0 - 20 °C

4: dimethylformamide / Ambient temperature

With potassium hydroxide; thionyl chloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00146a016

Reference yield:

: 636-78-2,97993-77-6
4-sulphobenzoic acid

: 89073-55-2
4-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]thiomorpholine

Guidance literature:: Multi-step reaction with 4 steps

1: ethyl <3-(dimethylamino)propyl>carbodiimide (EDAC) / H₂O

2: 30percent aq. KOH / 0.17 h / Heating

3: SOCl₂ / dimethylformamide / 0 - 20 °C

4: dimethylformamide / Ambient temperature

With potassium hydroxide; thionyl chloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00146a016