(S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

Base Information

Chemical Name:(S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate
CAS No.:1403943-75-8
Molecular Formula:C₂₀H₂₄N₄O₃
Molecular Weight:368.436
Hs Code.:

Synonyms:(S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

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Chemical Property of (S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

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Technology Process of (S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

There total 4 articles about (S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1403943-43-0
(S)-tert-bulyl 1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethylcarbamate

: 74-88-4
methyl iodide

: 1403943-75-8
(S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

Guidance literature:: (S)-tert-bulyl 1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethylcarbamate; With sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1403942-31-3
(S)-tert-butyl 1-oxo-1-(2-(phenylcarbamoyl)-1H-pyrrol-1-ylamino)propan-2-ylcarbamate

: 1403943-75-8
(S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 6 h / 80 °C

1.2: 1 h

1.3: 80 °C / Sealed

2.1: triethylamine / dichloromethane / 20 °C

3.1: sodium t-butanolate / tetrahydrofuran / 1 h / 20 °C

3.2: 20 °C

With triethylamine; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1403942-30-2
(S)-2-(1-aminoethyl)-3-phenylpyrrolo[1,2-f][1,2,4]triazin-4(3H)-one

: 1403943-75-8
(S)-tert-butyl methyl(1-(4-oxo-3-phenyl-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-2-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 20 °C

2.1: sodium t-butanolate / tetrahydrofuran / 1 h / 20 °C

2.2: 20 °C

With triethylamine; sodium t-butanolate; In tetrahydrofuran; dichloromethane;