N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

Base Information

Chemical Name:N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid
CAS No.:129053-09-4
Molecular Formula:C₁₄H₂₂N₂O₂
Molecular Weight:250.341
Hs Code.:

Synonyms:N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

Chemical Property:

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Technology Process of N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

There total 4 articles about N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 129053-08-3
2-(2'-Aminoethyl)-3-methoxy-N,N,α-trimethylbenzylamin

: 2258-42-6
formyl acetic anhydride

: 129053-09-4
N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

Guidance literature:: In dichloromethane; Ambient temperature;
DOI:10.1002/hlca.19900730323

Reference yield:

: 129052-92-2
N,N-dimethyl-α-(m-methoxyphenyl)ethylamine

: 129053-09-4
N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) BuLi / 1.) Et₂O, Hexan, 40 deg C, 3h, 2.) room temp., 2h

2: NaOAc / methanol / 16 h / Ambient temperature

3: LiAlH₄ / tetrahydrofuran / 2 h / Heating

4: 75 percent / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; sodium acetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.19900730323

Reference yield:

: 129052-93-3
(+/-)-N,N-dimethyl-α-(2-formyl-3-methoxyphenyl)ethylamine

: 129053-09-4
N-<2'-<2''-<1'''-(Dimethylamino)ethyl>-6''-methoxyphenyl>ethyl>formamid

Guidance literature:: Multi-step reaction with 3 steps

1: NaOAc / methanol / 16 h / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / 2 h / Heating

3: 75 percent / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; sodium acetate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.19900730323