(+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

Base Information

Chemical Name:(+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol
CAS No.:141947-67-3
Molecular Formula:C₄₂H₄₃FO₆
Molecular Weight:662.798
Hs Code.:

Synonyms:(+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

Chemical Property:

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Technology Process of (+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

There total 5 articles about (+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 129163-26-4,129261-63-8,142034-51-3,144540-16-9,146076-22-4
(+/-)-3,4,5,6-tetra-O-benzyl-1-O-(p-methoxybenzyl)-myo-inositol

: 141947-67-3
(+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 0 ℃; for 2h; 1) 2 h, 0 deg C, 2) 1 h, RT;

Reference yield:

: 26276-99-3
rac-1,4,5,6-tetra-O-benzyl-myo-inositol

: 141947-67-3
(+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) dibutyltin oxide, 2) CsF, KI / 1) toluene, reflux, 3 h, 2) DMF, RT, 24 h

2: 94 percent / (diethylamino)sulfur trifluoride (DAST) / CH₂Cl₂ / 2 h / 0 °C / 1) 2 h, 0 deg C, 2) 1 h, RT

With diethylamino-sulfur trifluoride; di(n-butyl)tin oxide; cesium fluoride; potassium iodide; In dichloromethane;

Reference yield:

: 100-39-0
benzyl bromide

: 141947-67-3
(+/-)-3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-1-O-(p-methoxybenzyl)-scyllo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / dimethylformamide

2: 80percent aq. acetic acid / 0.25 h / 100 °C

3: 1) dibutyltin oxide, 2) CsF, KI / 1) toluene, reflux, 3 h, 2) DMF, RT, 24 h

4: 94 percent / (diethylamino)sulfur trifluoride (DAST) / CH₂Cl₂ / 2 h / 0 °C / 1) 2 h, 0 deg C, 2) 1 h, RT

With diethylamino-sulfur trifluoride; sodium hydride; di(n-butyl)tin oxide; acetic acid; cesium fluoride; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;