Technology Process of 1,2,3,4-tetramethyl-5-(dimethylphenethylsilyl)cyclopenta-1,3-diene
There total 1 articles about 1,2,3,4-tetramethyl-5-(dimethylphenethylsilyl)cyclopenta-1,3-diene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1,2,3,4-tetramethylcyclopenta-1,3-diene;
With
n-butyllithium;
In
hexane;
dimethyl(2-phenylethyl)chlorosilane;
In
tetrahydrofuran;
DOI:10.1016/S0022-328X(02)01726-6
- Guidance literature:
-
With
LiBu; AgCl;
In
tetrahydrofuran; hexane;
(Ar); soln. of LiBu in hexane was added to TiCl4 in THF; mixt. was refluxed; LiBu was reacted under stirring with cyclopentadiene in THF for 24 h at room temp.; solns. were mixed; mixt. was refluxed for 30 h and stirred with AgCl at 40°C for 5 h; elem. anal.;
DOI:10.1016/S0022-328X(02)01726-6