Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

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Chemical Name:Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester
CAS No.:128963-06-4
Molecular Formula:C₃₀H₃₂ClF₂N₄O₁₄P
Molecular Weight:777.026
Hs Code.:

Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

Synonyms:Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

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Chemical Property of Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

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Technology Process of Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

There total 3 articles about Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 128963-05-3
Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

: 128963-06-4
Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

Guidance literature:: With nitrogen; fluorine; In acetic acid; for 0.5h; Ambient temperature;

Reference yield:

: 362-43-6
2',3'-O-isopropylideneuridine

: 128963-06-4
Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,2,4-triazole, TEA / 1.) dioxane, 30 min

2: 90 percent / F₂/N₂ (20/80) / acetic acid / 0.5 h / Ambient temperature

With 1,2,4-Triazole; TEA; nitrogen; fluorine; In acetic acid;

Reference yield:

: 772-79-2
4-chlorophenylphosphorodichloridate

: 128963-06-4
Phosphoric acid 4-chloro-phenyl ester bis-[(3aR,4R,6R,6aR)-6-(5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,2,4-triazole, TEA / 1.) dioxane, 30 min

2: 90 percent / F₂/N₂ (20/80) / acetic acid / 0.5 h / Ambient temperature

With 1,2,4-Triazole; TEA; nitrogen; fluorine; In acetic acid;