methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate

Base Information

Chemical Name:methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate
CAS No.:1215215-94-3
Molecular Formula:C₁₉H₁₃Br₂F₄NO₃
Molecular Weight:539.119
Hs Code.:

Synonyms:methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate

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Chemical Property of methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate

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Technology Process of methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate

There total 2 articles about methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261169-50-9
methyl 4-((hydroxyimino)methyl)-2-methylbenzoate

: 1350352-17-8
1,3-dibromo-2-fluoro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1215215-94-3
methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate

Guidance literature:: methyl 4-((hydroxyimino)methyl)-2-methylbenzoate; With N-chloro-succinimide; In 1,2-dimethoxyethane; at 80 ℃; for 2h;

1,3-dibromo-2-fluoro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene; With potassium hydrogencarbonate; In 1,2-dimethoxyethane; at 0 - 20 ℃; for 18h;

Reference yield:

: 1132701-15-5
1-(3,5-dibromo-4-fluorophenyl)-2,2,2-trifluoroethan-1-one

: 1215215-94-3
methyl 4-[5-(3,5-dibromo-4-fluorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

1.2: 18 h / 20 °C / Cooling with ice

2.1: N-chloro-succinimide / 1,2-dimethoxyethane / 2 h / 80 °C

2.2: 18 h / 0 - 20 °C

With N-chloro-succinimide; potassium tert-butylate; In tetrahydrofuran; 1,2-dimethoxyethane;