1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

Base Information

Chemical Name:1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate
CAS No.:607369-76-6
Molecular Formula:C₂₁H₂₃N₇O₄
Molecular Weight:437.458
Hs Code.:

Synonyms:1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

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Chemical Property of 1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

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Technology Process of 1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

There total 5 articles about 1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 607369-54-0
4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenol

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 607369-76-6
1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; at 20 ℃; for 18h;

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 607369-76-6
1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: trichlorophosphate / toluene / 16 h / 0 - 110 °C / Heating / reflux

2.1: sodium hydrogencarbonate / tetrahydrofuran; ethanol / 2 h / 20 - 80 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 2585.81 Torr

4.1: 0.42 h / 195 °C

5.1: hydrogenchloride; sodium nitrite / methanol; water / 1.5 h / 20 °C

5.2: 16 h / 110 °C / pH 11

6.1: boron tribromide / dichloromethane / 16 h / 0 - 20 °C

6.2: pH 14

7.1: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 18 h / 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; hydrogen; boron tribromide; sodium hydrogencarbonate; triphenylphosphine; sodium nitrite; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; toluene;

Reference yield:

: 14251-87-7
p. methoxy anilino-4 nitro-3 pyridine

: 607369-76-6
1,1-dimethylethyl [2-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)ethyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 2585.81 Torr

2.1: 0.42 h / 195 °C

3.1: hydrogenchloride; sodium nitrite / methanol; water / 1.5 h / 20 °C

3.2: 16 h / 110 °C / pH 11

4.1: boron tribromide / dichloromethane / 16 h / 0 - 20 °C

4.2: pH 14

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 18 h / 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; hydrogen; boron tribromide; triphenylphosphine; sodium nitrite; palladium 10% on activated carbon; In 1,4-dioxane; methanol; ethanol; dichloromethane; water;