6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

Base Information

Chemical Name:6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside
CAS No.:1200763-35-4
Molecular Formula:C₆₀H₆₉ClO₁₁
Molecular Weight:1001.65
Hs Code.:

Synonyms:6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

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Chemical Property of 6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

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Technology Process of 6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

There total 1 articles about 6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2009-83-8
6-chloro-1-hexanol

: 1200762-76-0
tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

: 1200763-35-4
6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

: 6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-α-D-galactopyranosyl)-1-β-D-glucopyranoside

Guidance literature:: 6-chloro-1-hexanol; tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside; In dichloromethane; at -55 - 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -55 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200901119

Reference yield: 73.0%

: O-(4,6-di-O-acetyl-2,3-di-O-benzyl-α/β-D-galactopyranosyl) trichloroacetimidate

: 1200763-35-4
6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

: C₈₄H₉₅ClO₁₈

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃;
DOI:10.1002/cbic.201200582

Reference yield:

: 1200763-56-9
4-methylphenyl 2,3-di-O-benzyl-4,6-O-di-tert-butylsilanediyl-1-thio-β-D-galactopyranoside

: 1200763-35-4
6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

: 1200763-60-5
6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-[2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-4,6-O-di-tert-butylsilylidene-α-D-galactopyranosyl)-β-D-galactopyranosyl]-1-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 2,3-di-O-benzyl-4,6-O-di-tert-butylsilanediyl-1-thio-β-D-galactopyranoside; 6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside; In dichloromethane; at -10 - 20 ℃; for 0.583333h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; Inert atmosphere;
DOI:10.1002/chem.200901119