tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

Base Information

Chemical Name:tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside
CAS No.:1200762-76-0
Molecular Formula:C₆₁H₆₄O₁₀S
Molecular Weight:989.239
Hs Code.:

Synonyms:tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

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Chemical Property of tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

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Technology Process of tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

There total 1 articles about tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1200764-33-5
C₆₁H₆₂O₁₀S

: 1200762-76-0
tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

Guidance literature:: C₆₁H₆₂O₁₀S; With triethylsilane; In dichloromethane; at -10 ℃; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1002/chem.200901119

Reference yield:

: 2009-83-8
6-chloro-1-hexanol

: 1200762-76-0
tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside

: 1200763-35-4
6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-glucopyranoside

: 6-chlorohexyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-α-D-galactopyranosyl)-1-β-D-glucopyranoside

Guidance literature:: 6-chloro-1-hexanol; tolyl 2,3,6-tri-O-benzyl-4-O-(2',3',6'-tri-O-benzyl-β-D-galactopyranosyl)-1-β-D-thioglucopyranoside; In dichloromethane; at -55 - 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -55 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200901119