methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate

Base Information

Chemical Name:methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate
CAS No.:1018071-76-5
Molecular Formula:C₂₁H₂₂BrNO₄S
Molecular Weight:464.38
Hs Code.:

Synonyms:methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate

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Chemical Property of methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate

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Technology Process of methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate

There total 1 articles about methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 124957-36-4
Methyl 3-acetoxy-2-methylene-3-phenylpropanoate

: 70-55-3
toluene-4-sulfonamide

: 513-31-5
2-bromoallyl bromide

: 1018071-76-5
methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate

Guidance literature:: Methyl 3-acetoxy-2-methylene-3-phenylpropanoate; With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; water; at 20 ℃;

toluene-4-sulfonamide; In tetrahydrofuran; water; at 20 ℃;

2-bromoallyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Further stages.;
DOI:10.1016/j.tetlet.2007.12.133

Reference yield: 68.0%

: 1018071-76-5
methyl 2-{[N-(2-bromoallyl)-4-methylphenylsulfonamido](phenyl)methyl}acrylate

: 1018071-84-5
5-methylene-2-phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 80 - 90 ℃; for 3h; Inert atmosphere;
DOI:10.1002/adsc.201300211