(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

Base Information

Chemical Name:(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide
CAS No.:84562-05-0
Molecular Formula:C₂₅H₂₁N₃O₇
Molecular Weight:475.458
Hs Code.:

Synonyms:(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

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Chemical Property of (4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

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Technology Process of (4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

There total 1 articles about (4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 23316-68-9
(2R,3R,4R,5R)-3,4-bis(benzoyloxy)-5-((benzoyloxy)methyl)tetrahydrofuran-2-carboxylic acid

: 84554-11-0
α-(1,6-dihydro-6-oxopyridazin-3-yl)methylamine

: 84562-05-0
(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

Guidance literature:: With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In acetonitrile; Ambient temperature;
DOI:10.1016/0008-6215(82)85041-6

Reference yield: 73.0%

: 84562-05-0
(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

: 98748-23-3,98748-24-4
2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-D-arabino-and-D-ribo-hexonamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 96h; under 760 Torr;
DOI:10.1039/P19850000621

Reference yield:

: 84562-05-0
(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-N-<(1,6-dihydro-6-oxopyridazin-3-yl)methyl>-4,5-dihydrofuran-2-carboxamide

: 84554-18-7,84562-08-3
C₂₅H₂₀ClN₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd-C / ethyl acetate / 760 Torr

2: 48 percent / POCl₃, pyridine / 1,2-dichloro-ethane / Heating

With pyridine; hydrogen; trichlorophosphate; palladium on activated charcoal; In ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(82)85041-6