octyl 2,6-dichloro-4-isonicotinate

Base Information

Chemical Name:octyl 2,6-dichloro-4-isonicotinate
CAS No.:309294-81-3
Molecular Formula:C₁₄H₁₉Cl₂NO₂
Molecular Weight:304.216
Hs Code.:

Synonyms:octyl 2,6-dichloro-4-isonicotinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octyl 2,6-dichloro-4-isonicotinate

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Technology Process of octyl 2,6-dichloro-4-isonicotinate

There total 1 articles about octyl 2,6-dichloro-4-isonicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 111-87-5
octanol

: 5398-44-7
2,6-dichloropyridine-4-carboxylic acid

: 309294-81-3
octyl 2,6-dichloro-4-isonicotinate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 5.5h;
DOI:10.1021/ol006318d

Reference yield: 86.0%

: 309294-81-3
octyl 2,6-dichloro-4-isonicotinate

: 101990-69-6
(2,6-dichloropyridin-4-yl)methanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 4h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201500026

Reference yield:

: 309294-81-3
octyl 2,6-dichloro-4-isonicotinate

: octyl 2,6-diethynyl-4-isonicotinate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / Pd₂(dibenzylideneacetone)3*CHCl₃; triphenylphosphine / triethylamine / 24 h / 70 °C

2: 33 percent / potassium carbonate / H₂O; tetrahydrofuran / 0.5 h / 20 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium carbonate; triphenylphosphine; In tetrahydrofuran; water; triethylamine; 1: Sonogashira coupling / 2: Substitution;
DOI:10.1021/ol006318d