O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

Base Information

Chemical Name:O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis
CAS No.:134935-53-8
Molecular Formula:C₁₈H₃₆N₂O₇S
Molecular Weight:424.559
Hs Code.:

O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis<carbamat>

Synonyms:O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

Suppliers and Price of O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

There total 1 articles about O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 134935-53-8
O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / pyridine / 2 h / 25 °C

2: 66 percent / CH₂Cl₂ / 5 h / 50 °C

3: 86 percent / triethylamine / acetonitrile / 25 °C

4: 85 percent / pyridine / 2 h / 25 °C

With pyridine; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/jlcr.1381

Reference yield:

: 134935-53-8
O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

: [3-(tert-butoxycarbonyl-{4-[2-(4-nitro-phenoxycarbonylamino)-acetylamino]-butyl}-amino)-propyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NH₃ / ethanol / 48 h / Ambient temperature

2: 1.) DCC, HOBT / 1.) CHCl₃, 0 deg C, 0.5 h, 2.) CHCl₃, from 0 deg C to RT

3: H₂ / 10 percent Pd/C / ethanol / 5 h / 760 Torr / Ambient temperature

4: Et₃N / tetrahydrofuran / 1 h / Ambient temperature

With ammonium hydroxide; hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm980431g

Reference yield:

: 134935-53-8
O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

: 221249-32-7
18-<(1,1-dimethylethoxy)carbonyl>-12-oxo-2,13,18,22-tetraazatricosanedioic acid, 23-(1,1-dimethylethyl) ester 1-phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NH₃ / ethanol / 48 h / Ambient temperature

2: 1.) DCC, HOBT / 1.) CHCl₃, 0 deg C, 0.5 h, 2.) CHCl₃, from 0 deg C to RT, overnight

With ammonium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethanol;
DOI:10.1021/jm980431g