N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

Base Information

Chemical Name:N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine
CAS No.:675587-83-4
Molecular Formula:C₂₀H₃₁N₅O₈
Molecular Weight:469.495
Hs Code.:

N<sup>ε</sup>-t-butyloxycarbonyl-N<sup>α</sup>-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

Synonyms:N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

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Chemical Property of N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

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Technology Process of N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

There total 2 articles about N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

: 2418-95-3
(S)-2-amino-6-(tert-butoxycarbonylamino)hexanoic acid

: 675587-65-2
N,N-dimethyl-2,4-dinitro-5-fluorobenzylamine

: 675587-83-4
N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

Guidance literature:: With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2003.12.001

Reference yield:

: 675587-66-3
N,N-dimethyl-2-nitro-5-fluorobenzylamine

: 675587-83-4
N^ε-t-butyloxycarbonyl-N^α-(2,4-dinitro-5-(dimethylaminomethyl)phenyl)-L-lysine

Guidance literature:: Multi-step reaction with 2 steps

1: 72.3 percent / HNO₃; H₂SO₄ / 2 h / 100 °C

2: 92.5 percent / NaHCO₃ / dimethylformamide; H₂O / 1 h / 20 °C

With sulfuric acid; nitric acid; sodium hydrogencarbonate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.12.001