Technology Process of tert-Butyl 2,4,6-triisopropylphenyl sulfoxide
There total 6 articles about tert-Butyl 2,4,6-triisopropylphenyl sulfoxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
1.) 0 deg C, 2.) 0.5 h, room temp.;
DOI:10.1021/jo00330a017
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85 percent / 1.) NaH / tetrahydrofuran / 1.) 0 deg C, 2.) 8h, room temp.
2: 59 percent / m-chloroperbenzoic acid / CHCl3 / 1.) 0 deg C, 2.) 0.5 h, room temp.
3: 6 percent / 380 °C / flash vacuum pyrolysis
4: 80 percent / pentane / 2 h / Ambient temperature
5: 70 percent / m-chloroperbenzoic acid / CHCl3 / 1.) 0 deg C, 2.) 0.5 h, room temp.
With
sodium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; chloroform; pentane;
DOI:10.1021/jo00330a017
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 59 percent / m-chloroperbenzoic acid / CHCl3 / 1.) 0 deg C, 2.) 0.5 h, room temp.
2: 6 percent / 380 °C / flash vacuum pyrolysis
3: 80 percent / pentane / 2 h / Ambient temperature
4: 70 percent / m-chloroperbenzoic acid / CHCl3 / 1.) 0 deg C, 2.) 0.5 h, room temp.
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform; pentane;
DOI:10.1021/jo00330a017
