6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 81098-42-2
• Molecular Formula: C₂₅H₂₄N₃O₄P₃
• Molecular Weight: 523.405

Synonyms:6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property:

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Technology Process of 6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 4 articles about 6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1-methyl-1-hydrido-3,3,5,5-tetrachlorocyclotriphosph(PV)azene (68351-74-6) + sodium phenoxide (139-02-6) → 6-Methyl-2,2,4,4-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-42-2)

Guidance literature:

In tetrahydrofuran; for 24h; Heating;

DOI:10.1021/ja00373a024

Reference yield: 27.0%

sodium 2,2,2-trifluoroethanolate (420-87-1) + 1,1'-dimethyl-3,3,3',3',5,5,5',5'-octaphenoxybi(cyclotriphosphazene) (81098-44-4) → 6-Methyl-2,2,4,4-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-42-2) + 2-Methyl-4,4,6,6-tetraphenoxy-2-(2,2,2-trifluoro-ethoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-45-5)

Guidance literature:

In tetrahydrofuran; for 48h; Heating;

DOI:10.1021/ja00373a024

Reference yield: 11.0%

sodium phenoxide (139-02-6) + 2-Butyl-4,4,6,6,4',4',6',6'-octachloro-2'-methyl-2λ5,4λ5,6λ5,2'λ5,4'λ5,6'λ5-[2,2']bi[[1,3,5,2,4,6]triazatriphosphininyl] (81098-55-7) → 6-Methyl-2,2,4,4-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-42-2) + 2-Methyl-2,4,4,6,6-pentaphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (75155-13-4) + 2-Butyl-2'-methyl-4,4,6,6,4',4',6',6'-octaphenoxy-2λ5,4λ5,6λ5,2'λ5,4'λ5,6'λ5-[2,2']bi[[1,3,5,2,4,6]triazatriphosphininyl] (81098-54-6)

Guidance literature:

In 1,4-dioxane; Heating;

DOI:10.1021/ja00373a024

upstream raw materials:

1-methyl-1-hydrido-3,3,5,5-tetrachlorocyclotriphosph(P^V)azene

sodium phenoxide

sodium 2,2,2-trifluoroethanolate

1,1'-dimethyl-3,3,3',3',5,5,5',5'-octaphenoxybi(cyclotriphosphazene)

Downstream raw materials:

2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

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