Technology Process of methyl 2-(1-dodecynyl)benzoate
There total 1 articles about methyl 2-(1-dodecynyl)benzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
for 16h;
Heating;
DOI:10.1021/jm00158a021
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 6h;
under 2068.6 Torr;
DOI:10.1021/jm00158a021
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 67 percent / H2 / 10percent Pd/C / ethyl acetate / 6 h / 2068.6 Torr
2: 1.) Mg, 3.) 3 N HCl
3: 45 percent / Jones reagent (CrO3, H2SO4) / H2O; acetone / 2 h / Ambient temperature
4: 100 percent / H2, H2SO4 / 10percent Pd/C / ethyl acetate / 0.13 h / 2585.7 Torr
With
hydrogenchloride; Jones reagent (CrO3, H2SO4); sulfuric acid; hydrogen; magnesium;
palladium on activated charcoal;
In
water; ethyl acetate; acetone;
DOI:10.1021/jm00158a021
