(RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

Base Information

Chemical Name:(RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine
CAS No.:124674-43-7
Molecular Formula:C₁₃H₁₄N₂O₂
Molecular Weight:230.266
Hs Code.:

Synonyms:(RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

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Chemical Property of (RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

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Technology Process of (RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

There total 6 articles about (RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₈N₂O₃

: 124674-43-7
(RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

Guidance literature:: With triethylamine; In toluene; iso-butanol; for 16h; Reflux;
DOI:10.1039/b904254g

Reference yield:

: 2577-48-2
methyl (2S)-pyrrolidine carboxylate

: 124674-43-7
(RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / acetonitrile / 20 h / 20 °C / Inert atmosphere

3: trichloroisocyanuric acid; water; hydrogenchloride / acetonitrile / 4 h / 20 °C / Inert atmosphere

4: sodium hydrogencarbonate / ethyl acetate; water / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; trichloroisocyanuric acid; water; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1002/ejoc.201301936

Reference yield:

: 19078-72-9
bromo(phenyl)acetyl chloride

: 124674-43-7
(RS) pyrrolo <1,2a> 3-phenyl 1,4-diketopiperazine

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / acetonitrile / 20 h / 20 °C / Inert atmosphere

3: trichloroisocyanuric acid; water; hydrogenchloride / acetonitrile / 4 h / 20 °C / Inert atmosphere

4: sodium hydrogencarbonate / ethyl acetate; water / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; trichloroisocyanuric acid; water; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1002/ejoc.201301936