Technology Process of C12H13NO4
There total 5 articles about C12H13NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 25 ℃;
for 44h;
DOI:10.1021/ja069371r
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / MgSO4 / CH2Cl2 / 25 °C
2: 91 percent / (S)-VAPOL; triphenyl borate / CCl4 / 24 h / 0 °C
3: 99 percent / anisole; triflic acid / 0.67 h / 25 °C
4: 98 percent / NaHCO3 / methanol / 2 h / 25 °C / ultrasound irradiation
5: 39 percent / Cu(OTf)2 / CH2Cl2 / 44 h / 25 °C
With
trifluorormethanesulfonic acid; copper(II) bis(trifluoromethanesulfonate); sodium hydrogencarbonate; magnesium sulfate; methoxybenzene;
(3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol;
In
methanol; tetrachloromethane; dichloromethane;
DOI:10.1021/ja069371r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 91 percent / (S)-VAPOL; triphenyl borate / CCl4 / 24 h / 0 °C
2: 99 percent / anisole; triflic acid / 0.67 h / 25 °C
3: 98 percent / NaHCO3 / methanol / 2 h / 25 °C / ultrasound irradiation
4: 39 percent / Cu(OTf)2 / CH2Cl2 / 44 h / 25 °C
With
trifluorormethanesulfonic acid; copper(II) bis(trifluoromethanesulfonate); sodium hydrogencarbonate; methoxybenzene;
(3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol;
In
methanol; tetrachloromethane; dichloromethane;
DOI:10.1021/ja069371r