(Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Base Information

Chemical Name:(Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal
CAS No.:1256752-72-3
Molecular Formula:C₂₈H₂₈O₃Si
Molecular Weight:440.614
Hs Code.:

Synonyms:(Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Suppliers and Price of (Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Chemical Property:

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Technology Process of (Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

There total 5 articles about (Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1256752-70-1
(Z)-3-(3-(1,3-dithian-2-yl)-3-methylbutylidene)-4-(triphenylsilyl)dihydrofuran-2(3H)-one

: 1256752-72-3
(Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Guidance literature:: With water; calcium carbonate; methyl iodide; In acetonitrile; at 60 ℃; Inert atmosphere;
DOI:10.1021/ol102278c

Reference yield:

: C₃₁H₃₆O₃S₂Si

: 1256752-72-3
(Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 48 h / -5 °C / Inert atmosphere

2: sodium methylate / tetrahydrofuran / 0 - 60 °C / Inert atmosphere

3: water; calcium carbonate; methyl iodide / acetonitrile / 60 °C / Inert atmosphere

With water; sodium methylate; triethylamine; calcium carbonate; methyl iodide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol102278c

Reference yield:

: C₃₂H₃₈O₅S₃Si

: 1256752-72-3
(Z)-4-(4-(triphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / tetrahydrofuran / 0 - 60 °C / Inert atmosphere

2: water; calcium carbonate; methyl iodide / acetonitrile / 60 °C / Inert atmosphere

With water; sodium methylate; calcium carbonate; methyl iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol102278c