(Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

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Chemical Name:(Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene
CAS No.:1370511-66-2
Molecular Formula:C₂₅H₂₈ClNO₂S
Molecular Weight:442.022
Hs Code.:

Synonyms:(Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

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Chemical Property of (Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

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Technology Process of (Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

There total 4 articles about (Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1354575-46-4
C₂₅H₂₉NO₃S

: 1370511-66-2
(Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

Guidance literature:: With iron(III) chloride; In dichloromethane; at 23 ℃; for 0.0166667h; under 760.051 Torr; Air;
DOI:10.1021/ol300434m

Reference yield:

: C₂₅H₂₇NO₃S

: 1370511-66-2
(Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 °C

2: iron(III) chloride / dichloromethane / 0.02 h / 23 °C / 760.05 Torr / Air

With iron(III) chloride; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1021/ol300434m

Reference yield:

: 3-Iodomethyl-5,5-dimethyl-cyclohex-2-enone

: 1370511-66-2
(Z)-4-(chloro(phenyl)methylene)-9,9-dimethyl-2-tosyl-2-azaspiro[4.5]dec-6-ene

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 20 °C

2: sodium tetrahydroborate / methanol / 0 °C

3: iron(III) chloride / dichloromethane / 0.02 h / 23 °C / 760.05 Torr / Air

With iron(III) chloride; sodium tetrahydroborate; In methanol; dichloromethane; acetone;
DOI:10.1021/ol300434m