prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

Base Information

Chemical Name:prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside
CAS No.:1384752-86-6
Molecular Formula:C₆₄H₆₀O₁₄
Molecular Weight:1053.17
Hs Code.:

Synonyms:prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

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Chemical Property of prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

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Technology Process of prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

There total 3 articles about prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1384752-82-2
C₃₀H₂₆O₉

: 1384752-77-5
1-ethynylcyclohexyl 2,3,4,6-tetra-O-benzyl α-D-mannopyranoside

: 1384752-86-6
prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

Guidance literature:: With gold(III) chloride; silver hexafluoroantimonate; In dichloromethane; acetonitrile; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c2cc32649c

Reference yield:

: C₁₄H₂₂O₆

: 1384752-86-6
prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

2: silver hexafluoroantimonate; gold(III) chloride / dichloromethane; acetonitrile / 8 h / 20 °C / Inert atmosphere

With gold(III) chloride; silver hexafluoroantimonate; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc32649c

Reference yield:

: 100-39-0
benzyl bromide

: 1384752-86-6
prop-2-yn-1-yl 2,3,6-tri-O-benzoyl 4-O-[2,3,4,6-tetra-O-benzyl α-D-mannopyranosyl] β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

2: silver hexafluoroantimonate; gold(III) chloride / dichloromethane; acetonitrile / 8 h / 20 °C / Inert atmosphere

With gold(III) chloride; silver hexafluoroantimonate; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc32649c