Technology Process of C32H53NO2Si
There total 3 articles about C32H53NO2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tert-butylhypochlorite; triethylamine;
In
diethyl ether; ethanol;
at -78 - 20 ℃;
Inert atmosphere;
Large scale;
DOI:10.1021/jo4026868
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere; Large scale
1.2: 1 h / -78 °C / Inert atmosphere; Large scale
2.1: pyridine; hydroxylamine hydrochloride / ethanol / 2 h / 20 °C / Inert atmosphere; Large scale
3.1: tert-butylhypochlorite; triethylamine / ethanol; diethyl ether / -78 - 20 °C / Inert atmosphere; Large scale
With
pyridine; n-butyllithium; tert-butylhypochlorite; hydroxylamine hydrochloride; triethylamine;
In
tetrahydrofuran; diethyl ether; ethanol; hexane;
DOI:10.1021/jo4026868
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; hydroxylamine hydrochloride / ethanol / 2 h / 20 °C / Inert atmosphere; Large scale
2: tert-butylhypochlorite; triethylamine / ethanol; diethyl ether / -78 - 20 °C / Inert atmosphere; Large scale
With
pyridine; tert-butylhypochlorite; hydroxylamine hydrochloride; triethylamine;
In
diethyl ether; ethanol;
DOI:10.1021/jo4026868