Technology Process of 4-Benzyloxy-6,6-dimethyl-2-prop-2-ynyloxymethyl-4,5,6,7-tetrahydro-benzofuran
There total 7 articles about 4-Benzyloxy-6,6-dimethyl-2-prop-2-ynyloxymethyl-4,5,6,7-tetrahydro-benzofuran which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
tetra(n-butyl)ammonium hydrogensulfate;
In
diethyl ether;
Ambient temperature;
DOI:10.1039/c39940001979
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / NaH / dimethylformamide / Ambient temperature
2: 95 percent / POCl3 / Ambient temperature
3: NaBH4 / ethanol / Ambient temperature
4: 98 percent / aq. NaOH / Bu4NHSO4 / diethyl ether / Ambient temperature
With
sodium hydroxide; sodium tetrahydroborate; sodium hydride; trichlorophosphate;
tetra(n-butyl)ammonium hydrogensulfate;
In
diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c39940001979
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1) aq. NaHCO3, 2) aq. H2SO4 / 1) CHCl3, r.t., 2) r.t.
2: 94 percent / NaBH4 / ethanol / Ambient temperature
3: 99 percent / NaH / dimethylformamide / Ambient temperature
4: 95 percent / POCl3 / Ambient temperature
5: NaBH4 / ethanol / Ambient temperature
6: 98 percent / aq. NaOH / Bu4NHSO4 / diethyl ether / Ambient temperature
With
sodium hydroxide; sodium tetrahydroborate; sulfuric acid; sodium hydride; sodium hydrogencarbonate; trichlorophosphate;
tetra(n-butyl)ammonium hydrogensulfate;
In
diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c39940001979
