1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

Base Information

Chemical Name:1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose
CAS No.:167612-63-7
Molecular Formula:C₃₁H₃₂O₆
Molecular Weight:500.591
Hs Code.:

Synonyms:1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

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Chemical Property of 1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

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Technology Process of 1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

There total 5 articles about 1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 25226-98-6
trans-cinnamaldehyde diethylacetal

: 167482-37-3
1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-β-D-psicopyranose

: 167612-62-6
1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'R)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

: 167612-63-7
1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; for 8h; Heating;
DOI:10.1021/jo00108a018

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 167612-63-7
1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: NH₄NO₃ / ethanol / Ambient temperature

2: 36 percent / pyridinium tosylate / benzene / 8 h / Heating

With ammonium nitrate; pyridinium p-toluenesulfonate; In ethanol; benzene;
DOI:10.1021/jo00108a018

Reference yield:

: 69351-19-5,18422-53-2
Shi's ketone

: 167612-63-7
1,2-O-Isopropylidene-3-O-(p-phenylbenzyl)-4,5-O-<(1'S)-trans-3'-phenyl-2'-propen-1'-yl>-β-D-psicopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / LiAlH₄ / tetrahydrofuran / 1 h / -78 °C

2: NaH / dimethylformamide / 1 h / Ambient temperature

3: 80percent aq. AcOH / 12 h / Ambient temperature

4: 36 percent / pyridinium tosylate / benzene / 8 h / Heating

With lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00108a018