1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine

Base Information

Chemical Name:1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine
CAS No.:1301628-71-6
Molecular Formula:C₃₆H₃₇N₃O₇
Molecular Weight:623.706
Hs Code.:

Synonyms:1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine

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Chemical Property of 1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine

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Technology Process of 1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine

There total 2 articles about 1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945382-94-5
C₂₆H₃₀O₇

: 126354-30-1
N-(5-methyl-2-oxo-1H-pyrimidin-4-yl)benzamide

: 1301628-71-6
1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine

Guidance literature:: C₂₆H₃₀O₇; N-(5-methyl-2-oxo-1H-pyrimidin-4-yl)benzamide; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 0.75h; Reflux;

With trimethylsulfonium triflate; In acetonitrile; at 0 - 20 ℃;
DOI:10.1021/jo200073q

Reference yield:

: 945382-92-3
4-C-allyl-3,5-di-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranose

: 1301628-71-6
1-[4-C-allyl-3,5-di-O-benzyl-2-O-acetyl-β-D-ribofuranosyl]-N4-benzoyl-5-methylcytosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluorormethanesulfonic acid; acetic acid / dichloromethane / 0.5 h / 0 °C

2.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.75 h / Reflux

2.2: 0 - 20 °C

With N,O-bis-(trimethylsilyl)-acetamide; trifluorormethanesulfonic acid; acetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jo200073q