C₁₁H₁₃BClN

Base Information

Chemical Name:C₁₁H₁₃BClN
CAS No.:1334174-18-3
Molecular Formula:C₁₁H₁₃BClN
Molecular Weight:205.495
Hs Code.:

Synonyms:C₁₁H₁₃BClN

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Chemical Property of C₁₁H₁₃BClN

Chemical Property:

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Technology Process of C₁₁H₁₃BClN

There total 1 articles about C₁₁H₁₃BClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1334174-16-1
C₁₃H₁₇BClN

: 1334174-18-3
C₁₁H₁₃BClN

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201103192

Reference yield: 48.0%

: 1334174-18-3
C₁₁H₁₃BClN

: 1334174-19-4
1-benzyl-2-chloro-1,2-azaborine

Guidance literature:: With palladium 10% on activated carbon; In cyclohexene; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201103192

Reference yield:

: 1334174-18-3
C₁₁H₁₃BClN

: C₁₃H₂₀BNO₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 4 h / -30 - 20 °C / Glovebox; Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / benzene / 4 h / 60 °C / 2327.23 Torr / Inert atmosphere; Glovebox; Sealed tube

3: dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Glovebox

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/om400697r