1-benzyl-2-methoxy-[1,2]azaborinane

Base Information

Chemical Name:1-benzyl-2-methoxy-[1,2]azaborinane
CAS No.:17150-65-1
Molecular Formula:C₁₂H₁₈BNO
Molecular Weight:203.092
Hs Code.:

Synonyms:1-benzyl-2-methoxy-[1,2]azaborinane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-2-methoxy-[1,2]azaborinane

Chemical Property:

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Technology Process of 1-benzyl-2-methoxy-[1,2]azaborinane

There total 3 articles about 1-benzyl-2-methoxy-[1,2]azaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₆BNO

: 17150-65-1
1-benzyl-2-methoxy-[1,2]azaborinane

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In benzene; at 60 ℃; for 4h; under 2327.23 Torr; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1021/om400697r

Reference yield:

: 67-56-1
methanol

: 17150-63-9
1-benzyl-1,2-azaborinane

: 17150-65-1
1-benzyl-2-methoxy-[1,2]azaborinane

Guidance literature:: DOI:10.1021/ja01000a054

Reference yield:

: 1334174-18-3
C₁₁H₁₃BClN

: 17150-65-1
1-benzyl-2-methoxy-[1,2]azaborinane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 4 h / -30 - 20 °C / Glovebox; Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / benzene / 4 h / 60 °C / 2327.23 Torr / Inert atmosphere; Glovebox; Sealed tube

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1021/om400697r