N⁴,N⁶-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine

Base Information

• Chemical Name: N⁴,N⁶-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine
• CAS No.: 356038-34-1
• Molecular Formula: C₂₄H₂₁IN₆O₅
• Molecular Weight: 600.372

Synonyms:N⁴,N⁶-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine

Chemical Property of N⁴,N⁶-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine

Chemical Property:

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Technology Process of N⁴,N⁶-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine

There total 3 articles about N⁴,N⁶-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

benzoyl chloride (98-88-4) + 1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine (356038-30-7) → N4,N6-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine (356038-34-1)

Guidance literature:

With pyridine; chloro-trimethyl-silane; at 20 ℃; for 24h;

DOI:10.1002/1522-2675(20010516)84:5<1048::AID-HLCA1048>3.0.CO;2-9

Reference yield: 75.0%

→ N4,N6-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine (356038-34-1)

Guidance literature:

Reference yield:

1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-4-isopropoxy-1H-pyrazolo[3,4-d]pyrimidin-6-amine (203180-17-0) → N4,N6-dibenzoyl-1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine (356038-34-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / NH₃; water / 96 h / 70 °C

2: 75 percent / Me₃SiCl; pyridine / 24 h / 20 °C

With pyridine; chloro-trimethyl-silane; ammonia; water;

DOI:10.1002/1522-2675(20010516)84:5<1048::AID-HLCA1048>3.0.CO;2-9

upstream raw materials:

benzoyl chloride

1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine

1-(2-deoxy-β-D-erythro-pentofuranosyl)-3-iodo-4-isopropoxy-1H-pyrazolo[3,4-d]pyrimidin-6-amine

Downstream raw materials:

N⁴,N⁶-dibenzoyl-1-[2-deoxy-5-O-(4,4'-dimethoxytrityl)-β-D-erythro-pentofuranosyl]-3-iodo-1H-pyrazolo[3,4-d]pyrimidine-4,6-diamine

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