8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Base Information

• Chemical Name: 8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside
• CAS No.: 110524-43-1
• Molecular Formula: C₆₅H₈₆O₁₄Si
• Molecular Weight: 1119.47

Synonyms:8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Chemical Property of 8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

There total 1 articles about 8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride (65827-59-0) + 8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside (106450-64-0) → 8-methoxycarbonyloctyl 2,6-di-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-α-D-mannopyranoside (110524-49-7) + 8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside (110524-43-1)

Guidance literature:

With silver trifluoromethanesulfonate; tetramethylurea; In 1,2-dichloro-ethane; at 20 ℃; for 2h;

DOI:10.1016/S0008-6215(00)90077-6

Reference yield: 86.0%

8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside (110524-43-1) → 8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside (110524-44-2)

Guidance literature:

With sodium methylate; In methanol; for 7h;

DOI:10.1016/S0008-6215(00)90077-6

upstream raw materials:

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride

8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

Downstream raw materials:

8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-α-D-mannopyranoside

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