8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside
CAS No.:106450-64-0
Molecular Formula:C₃₆H₅₆O₈Si
Molecular Weight:644.921
Hs Code.:

Synonyms:8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

There total 1 articles about 8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 110159-28-9
9-((2S,3S,4R,5R,6R)-4,5-Bis-benzyloxy-3-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-nonanoic acid methyl ester

: 106450-64-0
8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

Guidance literature:: In pyridine; for 15h;
DOI:10.1016/S0008-6215(00)90077-6

Reference yield: 69.0%

: 100-39-0
benzyl bromide

: 106450-64-0
8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

: 110524-41-9
8-methoxycarbonyloctyl 2,3,4-tri-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

Guidance literature:: With silver(l) oxide; In N,N-dimethyl-formamide; for 48h;
DOI:10.1016/S0008-6215(00)90077-6

Reference yield: 67.0%

: 65827-59-0
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride

: 106450-64-0
8-methoxycarbonyloctyl 3,4-di-O-benzyl-6-O-(tert-butyldimethylsilyl)-α-D-mannopyranoside

: 110524-49-7
8-methoxycarbonyloctyl 2,6-di-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-α-D-mannopyranoside

: 110524-43-1
8-methoxycarbonyloctyl 2-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In 1,2-dichloro-ethane; at 20 ℃; for 2h;
DOI:10.1016/S0008-6215(00)90077-6