p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt

Base Information

• Chemical Name: p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt
• CAS No.: 78272-50-1
• Molecular Formula: C₆H₁₃N*C₉H₉ClNO₄P
• Molecular Weight: 360.777

Synonyms:p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt

Chemical Property of p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt

Chemical Property:

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Technology Process of p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt

There total 3 articles about p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-chlorophenyl phosphorodichloridite (32666-92-5) → p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt (78272-50-1)

Guidance literature:

Multi-step reaction with 3 steps

1: trimethylamine / benzene; diethyl ether / 0.5 h / -10 - 0 °C

2: tert-BuOOH / benzene / 1 h / 25 °C

3: acetonitrile

With tert.-butylhydroperoxide; trimethylamine; In diethyl ether; acetonitrile; benzene;

DOI:10.1016/0040-4039(81)80013-5

Reference yield:

p-chlorophenyl-bis-(β-cyanoethyl)-phosphite (78272-46-5) → p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt (78272-50-1)

Guidance literature:

Multi-step reaction with 2 steps

1: tert-BuOOH / benzene / 1 h / 25 °C

2: acetonitrile

With tert.-butylhydroperoxide; In acetonitrile; benzene;

DOI:10.1016/0040-4039(81)80013-5

Reference yield:

p-chlorophenyl-bis-(β-cyanoethyl)-phosphate (78272-47-6) + cyclohexylamine (108-91-8,157973-60-9) → p-chlorophenyl-β-cyanoethylphosphoric acid cyclohexylammonium salt (78272-50-1)

Guidance literature:

In acetonitrile;

DOI:10.1016/0040-4039(81)80013-5

upstream raw materials:

p-chlorophenyl-bis-(β-cyanoethyl)-phosphate

cyclohexylamine

p-chlorophenyl phosphorodichloridite

p-chlorophenyl-bis-(β-cyanoethyl)-phosphite

Downstream raw materials:

O^5'-(4-methoxy-trityl)-[3']thymidylic acid 4-chloro-phenyl ester 2-cyano-ethyl ester

thymidine-3'-p-chlorophenyl-β-cyanoethyl-phosphate

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