1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

Base Information

Chemical Name:1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole
CAS No.:1446337-66-1
Molecular Formula:C₂₄H₃₂N₂O₃
Molecular Weight:396.53
Hs Code.:

Synonyms:1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

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Chemical Property of 1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

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Technology Process of 1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

There total 8 articles about 1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1446338-15-3
N-[2-(isobutylamino)-4-(3-methylbutoxy)phenyl]-2-(3-methoxyphenoxy)acetamide

: 1446337-66-1
1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

Guidance literature:: With acetic acid; at 100 ℃; for 3h;

Reference yield:

: 107-82-4
i-pentyl bromide

: 1446337-66-1
1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide monohydrate / ethanol / Reflux

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 2844.39 - 2999.54 Torr

4.1: tetrahydrofuran; methanol / 0.25 h / 20 °C

4.2: 20 °C

5.1: acetic acid / 3 h / 100 °C

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 2088-24-6
3-methoxyphenoxyacetic acid

: 1446337-66-1
1-isobutyl-2-(3-methoxyphenoxymethyl)-6-(3-methylbutoxy)-1H-benzimidazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 2844.39 - 2999.54 Torr

4.1: tetrahydrofuran; methanol / 0.25 h / 20 °C

4.2: 20 °C

5.1: acetic acid / 3 h / 100 °C

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate;