C₂₃H₂₈O₆

Base Information

Chemical Name:C₂₃H₂₈O₆
CAS No.:1426297-95-1
Molecular Formula:C₂₃H₂₈O₆
Molecular Weight:400.472
Hs Code.:

C<sub>23</sub>H<sub>28</sub>O<sub>6</sub>

Synonyms:C₂₃H₂₈O₆

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Chemical Property of C₂₃H₂₈O₆

Chemical Property:

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Technology Process of C₂₃H₂₈O₆

There total 13 articles about C₂₃H₂₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1426297-86-0
(3R,4R)-3-(4-benzyloxy-3-methoxybenzyl)-4-(3,4-diethoxybenzyl)dihydrofuran-2-one

: 1426297-95-1
C₂₃H₂₈O₆

Guidance literature:: With hydrogen; palladium(II) hydroxide; In methanol; for 20h; under 760.051 Torr;
DOI:10.1016/j.ejmech.2012.11.031

Reference yield:

: 83459-29-4
(3,4-diethoxyphenyl)methanol

: 1426297-95-1
C₂₃H₂₈O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

2.2: 25 h / 0 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 °C / Reflux

4.1: Amano lipase-PS / tetrahydrofuran; di-isopropyl ether / 2 h / 20 °C / Enzymatic reaction

5.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

6.1: dimethyl sulfoxide / 3 h / 90 °C

7.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 °C

8.1: water; sodium hydroxide / 5 h / Reflux

9.1: hydrogenchloride / tetrahydrofuran; water / 50 h / 20 °C

10.1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 0.5 h / -78 °C

10.2: 21 h / 20 °C

11.1: hydrogen; palladium(II) hydroxide / methanol / 20 h / 760.05 Torr

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; lithium hydroxide monohydrate; Amano lipase-PS; water; hydrogen; palladium(II) hydroxide; sodium hydride; triethylamine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; di-isopropyl ether; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2012.11.031

Reference yield:

: 1426298-00-1
(R)-acetic acid 3-(3,4-diethoxyphenyl)-2-hydroxymethylpropyl ester

: 1426297-95-1
C₂₃H₂₈O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

2.1: dimethyl sulfoxide / 3 h / 90 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 °C

4.1: water; sodium hydroxide / 5 h / Reflux

5.1: hydrogenchloride / tetrahydrofuran; water / 50 h / 20 °C

6.1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 0.5 h / -78 °C

6.2: 21 h / 20 °C

7.1: hydrogen; palladium(II) hydroxide / methanol / 20 h / 760.05 Torr

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hydroxide monohydrate; water; hydrogen; palladium(II) hydroxide; triethylamine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2012.11.031