2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

Base Information

Chemical Name:2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride
CAS No.:68967-74-8
Molecular Formula:C₁₃H₂₁IN₂O₃S*ClH
Molecular Weight:448.753
Hs Code.:

Synonyms:2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

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Chemical Property of 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

Chemical Property:

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Technology Process of 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

There total 3 articles about 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68967-73-7
(5-tert-Butyl-2-ethylsulfamoyloxy-3-iodo-benzyl)-carbamic acid tert-butyl ester

: 68967-74-8
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 20 - 25 ℃; for 3h; Yield given;
DOI:10.1021/jm00348a024

Reference yield:

: 58456-91-0
2-aminomethyl-4-tert-butyl-6-iodophenol

: 68967-74-8
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Et₃N / tetrahydrofuran; H₂O / 24 h / 60 - 65 °C

2: Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

3: conc. HCl / ethanol / 3 h / 20 - 25 °C

With hydrogenchloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00348a024

Reference yield:

: 68967-65-7
1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

: 68967-74-8
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl N-ethylsulfamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

2: conc. HCl / ethanol / 3 h / 20 - 25 °C

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm00348a024