C₂₀H₂₂F₂N₃O₃P

Base Information

Chemical Name:C₂₀H₂₂F₂N₃O₃P
CAS No.:1408232-37-0
Molecular Formula:C₂₀H₂₂F₂N₃O₃P
Molecular Weight:421.384
Hs Code.:

C<sub>20</sub>H<sub>22</sub>F<sub>2</sub>N<sub>3</sub>O<sub>3</sub>P

Synonyms:C₂₀H₂₂F₂N₃O₃P

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Chemical Property of C₂₀H₂₂F₂N₃O₃P

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Technology Process of C₂₀H₂₂F₂N₃O₃P

There total 5 articles about C₂₀H₂₂F₂N₃O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 18653-75-3
2-(2'-pyridyl)imidazole

: 174678-80-9
diethyl [(4-α-bromomethyl)phenyldifluoromethyl]-phosphonate

: 1408232-37-0
C₂₀H₂₂F₂N₃O₃P

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; butan-1-ol; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic301884j

Reference yield:

: 79158-40-0
diethyl hydroxy(p-tolyl)methylphosphonate

: 1408232-37-0
C₂₀H₂₂F₂N₃O₃P

Guidance literature:: Multi-step reaction with 4 steps

1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere; Schlenk technique

2: dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

3: 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / Inert atmosphere; Schlenk technique; Reflux

4: potassium tert-butylate / N,N-dimethyl-formamide; butan-1-ol / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With 2,2'-azobis(isobutyronitrile); potassium tert-butylate; Dess-Martin periodane; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/ic301884j

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1408232-37-0
C₂₀H₂₂F₂N₃O₃P

Guidance literature:: Multi-step reaction with 5 steps

1: N,N,N',N'-tetramethylguanidine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Schlenk technique

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere; Schlenk technique

3: dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

4: 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / Inert atmosphere; Schlenk technique; Reflux

5: potassium tert-butylate / N,N-dimethyl-formamide; butan-1-ol / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With 2,2'-azobis(isobutyronitrile); potassium tert-butylate; Dess-Martin periodane; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/ic301884j