1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

Base Information

Chemical Name:1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one
CAS No.:111708-81-7
Molecular Formula:C₁₉H₁₇Cl₂NO₃S
Molecular Weight:410.321
Hs Code.:

Synonyms:1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

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Chemical Property of 1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

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Technology Process of 1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

There total 4 articles about 1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 79-36-7
dichloroacethyl chloride

: 111708-72-6
2,3-dihydro-7,8-dimethoxy-5-phenyl-1,4-benzothiazepine

: 111708-81-7
1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

Guidance literature:: With triethylamine; In benzene; for 1h; Heating;
DOI:10.1139/v87-027

Reference yield:

: 111708-66-8
2-((3,4-dimethoxyphenyl)thio)ethan-1-amine hydrochloride

: 111708-81-7
1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / 0.5 h

2: 36.7 percent / POCl₃ / 3 h / Heating

3: 95 percent / triethylamine / benzene / 1 h / Heating

With pyridine; triethylamine; trichlorophosphate; In benzene;
DOI:10.1139/v87-027

Reference yield:

: 111708-69-1
2'-benzoylaminoethyl-3,4-dimethoxyphenyl sulfide

: 111708-81-7
1,1-Dichloro-7,8-dimethoxy-9b-phenyl-1,3,4,9b-tetrahydro-5-thia-2a-aza-benzo[a]cyclobuta[c]cyclohepten-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 36.7 percent / POCl₃ / 3 h / Heating

2: 95 percent / triethylamine / benzene / 1 h / Heating

With triethylamine; trichlorophosphate; In benzene;
DOI:10.1139/v87-027