2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

Base Information

Chemical Name:2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide
CAS No.:1208130-65-7
Molecular Formula:C₁₆H₂₁Cl₂N₇O₆
Molecular Weight:478.292
Hs Code.:

Synonyms:2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

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Technology Process of 2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

There total 6 articles about 2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

: C₁₇H₂₂Cl₂N₆O₆

: 1208130-65-7
2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

Guidance literature:: With hydroxylamine potassium salt; In methanol;
DOI:10.1007/s00044-017-1999-2

Reference yield:

: 74-79-3,25212-18-4
L-arginine

: 1208130-65-7
2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; sulfuric acid

2: acetyl chloride

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / -5 °C

4: hydroxylamine potassium salt / methanol

With hydroxylamine potassium salt; sulfuric acid; nitric acid; benzotriazol-1-ol; acetyl chloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol;
DOI:10.1007/s00044-017-1999-2

Reference yield:

: 2149-70-4,13855-78-2,38733-00-5
N-nitro-L-arginine

: 1208130-65-7
2,4-dichloro-N-((S)-1-((S)-1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-ylamino)-1-oxopropan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride

2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / -5 °C

3: hydroxylamine potassium salt / methanol

With hydroxylamine potassium salt; benzotriazol-1-ol; acetyl chloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol;
DOI:10.1007/s00044-017-1999-2