6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

Base Information

Chemical Name:6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine
CAS No.:1266156-31-3
Molecular Formula:C₂₄H₁₉N₅O
Molecular Weight:393.448
Hs Code.:

Synonyms:6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

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Chemical Property of 6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

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Technology Process of 6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

There total 3 articles about 6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1266161-04-9
N-(3-(6-chloro-5-cyano-4-(4-phenoxyphenyl)pyridin-2-yl)phenyl)acetamide

: 1266156-31-3
6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

: 1266156-30-2
N-(3-(3-amino-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyridin-6-yl)phenyl)acetamide

Guidance literature:: With hydrazine; In water; isopropyl alcohol; at 160 ℃; for 1h; Microwave irradiation;

Reference yield:

: trans-3-cyano-6-oxo-4-(4-phenoxyphenyl)-5-(pyridinium-1-yl)-1,4,5,6-tetrahydropyridin-2-olate

: 1266156-31-3
6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

: 1266156-30-2
N-(3-(3-amino-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyridin-6-yl)phenyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 24 h / 135 °C

2: potassium phosphate monohydrate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C / Inert atmosphere

3: hydrazine / isopropyl alcohol; water / 1 h / 160 °C / Microwave irradiation

With potassium phosphate monohydrate; hydrazine; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; isopropyl alcohol; 2: Suzuki Coupling;

Reference yield:

: 1266160-98-8
2,6-dichloro-4-(4-phenoxyphenyl)nicotinonitrile

: 1266156-31-3
6-(3-aminophenyl)-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyr idin-3-amine

: 1266156-30-2
N-(3-(3-amino-4-(4-phenoxyphenyl)-1H-pyrazolo[3,4-b]pyridin-6-yl)phenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate monohydrate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C / Inert atmosphere

2: hydrazine / isopropyl alcohol; water / 1 h / 160 °C / Microwave irradiation

With potassium phosphate monohydrate; hydrazine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; isopropyl alcohol; 1: Suzuki Coupling;