4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline

Base Information

• Chemical Name: 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline
• CAS No.: 1564287-27-9
• Molecular Formula: C₂₉H₃₃Br₂NSi
• Molecular Weight: 583.481

Synonyms:4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline

Chemical Property of 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline

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Technology Process of 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline

There total 3 articles about 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

1,4-bromoiodobenzene (589-87-7) + (R,Z)-4,4,5,5-tetramethyl-2-(2-methylhex-4-en-3-yl)-1,3,2-dioxaborolane → 5-(4-(10H-phenoxazin-10-yl)phenyl)thiophene-2-carbaldehyde (1507401-59-3) + bis[4-(3,6-di-tert-butylcarbazole)phenyl] sulfone (1396165-20-0) + 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline (1564287-27-9)

Guidance literature:

With 18-crown-6 ether; copper; potassium carbonate; In N,N-dimethyl-formamide; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/ja5040073

Reference yield: 31.0%

1,4-bromoiodobenzene (589-87-7) + (R,Z)-4,4,5,5-tetramethyl-2-(2-methylhex-4-en-3-yl)-1,3,2-dioxaborolane → 5-(4-(10H-phenoxazin-10-yl)phenyl)thiophene-2-carbaldehyde (1507401-59-3) + bis[4-(3,6-di-tert-butylcarbazole)phenyl] sulfone (1396165-20-0) + 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline (1564287-27-9) + C26H16N2O3S (1507401-60-6) + C13H17Br + N-(4′-bromo-3-methylbiphenyl-2-yl)formamide (1608474-10-7)

Guidance literature:

With 18-crown-6 ether; copper; potassium carbonate; In N,N-dimethyl-formamide; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/ja5040073

Reference yield: 31.0%

1,4-bromoiodobenzene (589-87-7) + (R,Z)-4,4,5,5-tetramethyl-2-(2-methylhex-4-en-3-yl)-1,3,2-dioxaborolane → 5-(4-(10H-phenoxazin-10-yl)phenyl)thiophene-2-carbaldehyde (1507401-59-3) + bis[4-(3,6-di-tert-butylcarbazole)phenyl] sulfone (1396165-20-0) + 4-bromo-N-(4-bromophenyl)-N-(4-((triisopropylsilyl)ethynyl)phenyl)aniline (1564287-27-9) + C26H16N2O3S (1507401-60-6) + C13H17Br + N-(4′-bromo-3-methylbiphenyl-2-yl)formamide (1608474-10-7) + (R,E)-1-bromo-4-(5-methylhex-3-en-2-yl)benzene

Guidance literature:

With 18-crown-6 ether; copper; potassium carbonate; In N,N-dimethyl-formamide; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/ja5040073

upstream raw materials:

1,4-bromoiodobenzene

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