<2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

Base Information

Chemical Name:<2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester
CAS No.:147753-50-2
Molecular Formula:C₂₇H₂₄O₆
Molecular Weight:444.484
Hs Code.:

<2-(methoxycarbonyl)-6,11-dihydrodibenz<b,e>oxepin-11-yl>benzoylacetic acid ethyl ester

Synonyms:<2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

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Chemical Property of <2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

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Technology Process of <2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

There total 1 articles about <2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 79670-00-1
methyl 11-methoxy-6,11-dihydrodibenz[b,e]oxepin-2-carboxylate

: 147753-50-2
<2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

Guidance literature:: With titanium tetrachloride; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1248/cpb.41.36

Reference yield: 42.0%

: 147753-50-2
<2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

: 147753-52-4
11-phenacyl-6,11-dihydrodibenzoxepin-2-carboxylic acid methyl ester

Guidance literature:: With water; sodium chloride; In dimethyl sulfoxide; at 150 - 160 ℃; for 8h;
DOI:10.1248/cpb.41.36

Reference yield:

: 147753-50-2
<2-(methoxycarbonyl)-6,11-dihydrodibenzoxepin-11-yl>benzoylacetic acid ethyl ester

: 11-phenacyl-6,11-dihydrodibenzoxepin-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / NaCl, H₂O / dimethylsulfoxide / 8 h / 150 - 160 °C

2: 72 percent / 10N aq. NaOH / methanol; dioxane / 6 h / Heating

With sodium hydroxide; water; sodium chloride; In 1,4-dioxane; methanol; dimethyl sulfoxide;
DOI:10.1248/cpb.41.36