2-(Boc-amino)-3-buten-1-ol

Base Information

Chemical Name:2-(Boc-amino)-3-buten-1-ol
CAS No.:169324-82-7
Molecular Formula:C9H17 N O3
Molecular Weight:187.24
Hs Code.:2924199090
DSSTox Substance ID:DTXSID80542776
Nikkaji Number:J1.323.330F
Mol file:169324-82-7.mol

Synonyms:2-(boc-amino)-3-buten-1-ol;169324-82-7;TERT-BUTYL N-(1-HYDROXYBUT-3-EN-2-YL)CARBAMATE;tert-Butyl (1-hydroxybut-3-en-2-yl)carbamate;MFCD19688626;(R)-2-(Boc-amino)-3-buten-1-ol;(R)-tert-butyl 1-hydroxybut-3-en-2-ylcarbamate;SCHEMBL6167799;2-(boc-amino)-3-buen-1-ol;DAlc2-H_000056;DTXSID80542776;HYVYNSIWYIWTCK-UHFFFAOYSA-N;SB44512;SB44591;n-(tert-butoxycarbonyl)-2-vinylglycinol;BCB04_000219;SY036371;t-butyl 1-hydroxy-3-buten-2-yl-carbamate;EN300-717974

Suppliers and Price of 2-(Boc-amino)-3-buten-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(Boc-amino)-3-buten-1-ol

Chemical Property:

PSA：58.56000
LogP:1.44890
XLogP3:0.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:187.12084340
Heavy Atom Count:13
Complexity:184

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC(CO)C=C

Technology Process of 2-(Boc-amino)-3-buten-1-ol

There total 7 articles about 2-(Boc-amino)-3-buten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 451502-79-7
tert-butyl 2-oxo-4-vinyloxazolidinone-3-carboxylate

: 169324-82-7
N-tert-butoxycarbonyl-N-(1-hydroxymethyl-2-propenyl)amine

Guidance literature:: With caesium carbonate; In methanol;
DOI:10.1002/1521-3773(20020503)41:9<1614::AID-ANIE1614>3.0.CO;2-5

Reference yield: 71.0%

: 267668-24-6
N-tert-butyloxycarbonyl-N-(1-hydroxymethyl-2-propenyl)benzenesulfenamide

: 169324-82-7
N-tert-butoxycarbonyl-N-(1-hydroxymethyl-2-propenyl)amine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 1h; Heating;
DOI:10.1021/jo991569p

Reference yield:

: 115148-32-8
3-(4-methoxyphenyl)-4-vinyloxazolidin-2-one

: 169324-82-7
N-tert-butoxycarbonyl-N-(1-hydroxymethyl-2-propenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / ceric ammonium nitrate / acetonitrile; H₂O

2: 88 percent / triethylamine / CH₂Cl₂

3: 88 percent / Cs₂CO₃ / methanol

With ammonium cerium(IV) nitrate; caesium carbonate; triethylamine; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/1521-3773(20020503)41:9<1614::AID-ANIE1614>3.0.CO;2-5