ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

Base Information

Chemical Name:ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate
CAS No.:1313892-49-7
Molecular Formula:C₂₂H₂₃BrO₆
Molecular Weight:463.325
Hs Code.:

Synonyms:ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

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Technology Process of ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

There total 6 articles about ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: ethyl (E)-4-(4-(3-(5-bromo-2-methoxy-4-(tetrahydro-2H-pyran-2-yloxy)phenyl)acryloyl)-phenoxy)butanoate

: 1313892-49-7
ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2011.04.057

Reference yield:

: 1313891-05-2
5-bromo-2-hydroxy-4-(tetrahydro-2H-pyran-2-yloxy)benzaldehyde

: 1313892-49-7
ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 10 h / 20 °C

2: potassium hydroxide / ethanol; water / 48 h / 20 °C

3: potassium carbonate / acetone / 20 °C

4: hydrogenchloride; water / tetrahydrofuran; methanol / 20 °C

With hydrogenchloride; water; potassium carbonate; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; water; acetone;
DOI:10.1016/j.bmcl.2011.04.057

Reference yield:

: 1313892-43-1
(E)-3-(5-bromo-2-methoxy-4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-1-(4-hydroxyphenyl)prop-2-en-1-one

: 1313892-49-7
ethyl (E)-4-(4-(3-(5-bromo-4-hydroxy-2-methoxyphenyl)acryloyl)phenoxy)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 20 °C

2: hydrogenchloride; water / tetrahydrofuran; methanol / 20 °C

With hydrogenchloride; water; potassium carbonate; In tetrahydrofuran; methanol; acetone;
DOI:10.1016/j.bmcl.2011.04.057