N-[2-(Nitroso-phenyl-amino)ethyl]-N-phenyl-nitrous amide

Base Information

• Chemical Name: N-[2-(Nitroso-phenyl-amino)ethyl]-N-phenyl-nitrous amide
• CAS No.: 4979-29-7
• Molecular Formula: C14H14 N4 O2
• Molecular Weight: 270.291
• NSC Number: 137905
• DSSTox Substance ID: DTXSID30964404
• Wikidata: Q82946386
• Mol file: 4979-29-7.mol

Synonyms:4979-29-7;NSC137905;DTXSID30964404;N-[2-(NITROSO-PHENYL-AMINO)ETHYL]-N-PHENYL-NITROUS AMIDE;NSC-137905;N,N'-Ethane-1,2-diylbis(N-phenylnitrous amide)

Chemical Property of N-[2-(Nitroso-phenyl-amino)ethyl]-N-phenyl-nitrous amide

Chemical Property:

• Boiling Point: 496.1±41.0 °C(Predicted)
• PKA: -2.18±0.50(Predicted)
• Flash Point: 253.8oC
• PSA: 65.34000
• Density: 1.19±0.1 g/cm3(Predicted)
• LogP: 3.36240
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 270.11167570
• Heavy Atom Count: 20
• Complexity: 272

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N(CCN(C2=CC=CC=C2)N=O)N=O

Technology Process of N-[2-(Nitroso-phenyl-amino)ethyl]-N-phenyl-nitrous amide

There total 3 articles about N-[2-(Nitroso-phenyl-amino)ethyl]-N-phenyl-nitrous amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-diphenylethylenediamine (150-61-8) → N,N'-dinitroso-N,N'-diphenyl-ethylenediamine (4979-29-7)

Guidance literature:

With hydrogenchloride; water; sodium nitrite;

Reference yield:

N-methyl-N-nitrosoaniline (614-00-6) → N,N'-dinitroso-N,N'-diphenyl-ethylenediamine (4979-29-7)

Guidance literature:

Multistep reaction; (i) LDA, THF, (ii) I₂;

DOI:10.1002/hlca.19780610512

Reference yield:

1,2-bis-(N-phenyl-hydrazino)-ethane (50710-37-7) + cis-nitrous acid (7782-77-6) → N,N'-dinitroso-N,N'-diphenyl-ethylenediamine (4979-29-7)

Guidance literature:

upstream raw materials:

N,N'-diphenylethylenediamine

N-methyl-N-nitrosoaniline

1,2-bis-(N-phenyl-hydrazino)-ethane

cis-nitrous acid

Downstream raw materials:

N,N'-bis-(4-nitroso-phenyl)-ethylenediamine

N,N'-bis(4-aminophenyl)ethane-1,2-diamine

N,N'-diphenylethylenediamine