4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

Base Information

Chemical Name:4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane
CAS No.:1276543-59-9
Molecular Formula:C₂₂H₃₅N₅O₄
Molecular Weight:433.551
Hs Code.:

Synonyms:4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

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Chemical Property of 4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

Chemical Property:

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Technology Process of 4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

There total 8 articles about 4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276543-58-8
4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

: 1276543-59-9
4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

Guidance literature:: In CF₃CO₂H; dichloromethane;

Reference yield:

: 7598-70-1
diethyl 2-(4-nitrobenzyl)malonate

: 1276543-59-9
4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / dichloromethane; ethanol

2: pyridine

3: sodium carbonate / aq NaOH; dichloromethane; toluene

4: palladium-carbon / ethanol

5: dichloromethane; CF₃CO₂H

With sodium tetrahydroborate; sodium carbonate; palladium-carbon; In pyridine; CF₃CO₂H; aq NaOH; ethanol; dichloromethane; toluene;

Reference yield:

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 1276543-59-9
4,10-bis-(carboxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[5.5.3]pentadecane

Guidance literature:: Multi-step reaction with 6 steps

1: NaOH / chloroform; benzyl chloroformate

2: acetonitrile; sodium carbonate

3: palladium-carbon / ethanol

4: sodium carbonate / aq NaOH; dichloromethane; toluene

5: palladium-carbon / ethanol

6: dichloromethane; CF₃CO₂H

With NaOH; sodium carbonate; palladium-carbon; In CF₃CO₂H; aq NaOH; ethanol; dichloromethane; chloroform; sodium carbonate; benzyl chloroformate; toluene; acetonitrile;