4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

Base Information

Chemical Name:4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane
CAS No.:1276543-58-8
Molecular Formula:C₃₀H₅₁N₅O₄
Molecular Weight:545.766
Hs Code.:

Synonyms:4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

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Chemical Property of 4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

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Technology Process of 4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

There total 10 articles about 4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1276543-57-7
4,10-bis-(carbo-tert-butoxymethyl)-14-(4-nitrobenzyl)-1,4,7,10-tetraazabicyclo[5. 5.3]pentadecane

: 1276543-58-8
4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 12h;

Reference yield:

: 7598-70-1
diethyl 2-(4-nitrobenzyl)malonate

: 1276543-58-8
4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / ethanol / 16 h / Reflux

2: pyridine / 10 h / 0 - 20 °C

3: sodium carbonate / toluene / 144 h / Reflux

4: hydrogen / palladium 10% on activated carbon / ethanol / 12 h / 20 °C

With pyridine; sodium tetrahydroborate; hydrogen; sodium carbonate; palladium 10% on activated carbon; In ethanol; toluene;

Reference yield:

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 1276543-58-8
4,10-bis-(carbo-tert-butoxymethyl)-14-(4-aminobenzyl)-1,4,7,10-tetraazabicyclo[ 5.5.3]pentadecane

Guidance literature:: Multi-step reaction with 6 steps

1: chloroform / 10 h / 0 - 20 °C

2: sodium hydroxide / water

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 10 h / 60 °C

4: hydrogen / palladium 10% on activated carbon / ethanol / 12 h / 20 °C

5: sodium carbonate / toluene / 144 h / Reflux

6: hydrogen / palladium 10% on activated carbon / ethanol / 12 h / 20 °C

With hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; palladium 10% on activated carbon; In ethanol; chloroform; water; toluene; acetonitrile;